Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod

›› 2012, Vol. 20 ›› Issue (1): 89-94.

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Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod

NING Zhanglei¹, CHANG Zhidong¹, LI Wenjun¹, SUN Changyan¹, ZHANG Jinghua², LIU Yang²

1. School of Chemical and Biological Engineering, University of Science and Technology Beijing, Beijing 100083, China;
2. Beijing Centre for Physical & Chemical Analysis, Beijing 100089, China

Received:2010-05-30 Revised:2010-11-09 Online:2012-05-03 Published:2012-02-28
Supported by:
Supported by the National Natural Science Foundation of China (20876157);the Fundamental Research Funds for the Central Universities (FRF-BR-10-002A)

Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod

宁张磊¹, 常志东¹, 李文军¹, 孙长艳¹, 张经华², 刘洋²

1. School of Chemical and Biological Engineering, University of Science and Technology Beijing, Beijing 100083, China;
2. Beijing Centre for Physical & Chemical Analysis, Beijing 100089, China

通讯作者: CHANG Zhidong,E-mail:zdchang@ustb.edu.cn;LI Wenjun,E-mail:wjli@sas.ustb.edu.cn
基金资助:
Supported by the National Natural Science Foundation of China (20876157);the Fundamental Research Funds for the Central Universities (FRF-BR-10-002A)

Abstract

Abstract: One-dimensional strontium hydroxyapatite(Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method.The products were characterized via X-ray diffraction(XRD),Fourier transform infrared(FT-IR),cold field emission scanning electron microscopy(FESEM),transmission electron microscopy(TEM),photoluminescence(PL) excitation and emission spectra.The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders.A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated.Moreover,the as-obtained Sr-HAp samples showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders.The possible luminescent mechanism of the Sr-HAp samples was discussed.

Key words: strontium hydroxyapatite, biomaterial, solvothermal synthesis, optical performance

摘要： One-dimensional strontium hydroxyapatite(Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method.The products were characterized via X-ray diffraction(XRD),Fourier transform infrared(FT-IR),cold field emission scanning electron microscopy(FESEM),transmission electron microscopy(TEM),photoluminescence(PL) excitation and emission spectra.The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders.A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated.Moreover,the as-obtained Sr-HAp samples showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders.The possible luminescent mechanism of the Sr-HAp samples was discussed.

关键词: strontium hydroxyapatite, biomaterial, solvothermal synthesis, optical performance

CLC Number:

TB383.1

NING Zhanglei, CHANG Zhidong, LI Wenjun, SUN Changyan, ZHANG Jinghua, LIU Yang. Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod[J]. , 2012, 20(1): 89-94.

宁张磊, 常志东, 李文军, 孙长艳, 张经华, 刘洋. Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod[J]. , 2012, 20(1): 89-94.

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Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod

Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod

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