A covalently integrated ZIF-8/polyamide acid mixed matrix membrane with superior gas separation performance

doi:10.1016/j.cjche.2024.06.031

Chinese Journal of Chemical Engineering ›› 2024, Vol. 76 ›› Issue (12): 30-41.DOI: 10.1016/j.cjche.2024.06.031

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A covalently integrated ZIF-8/polyamide acid mixed matrix membrane with superior gas separation performance

Guozhen Li^1,2, Shiqi Ling^1,3, Yuhui Cui¹, Shilong Dong¹, Tianyin Liu², Ting Li², Siyu Pang¹, Peiyong Qin¹

1. National Energy Research and Development Center for Biorefinery, College of Life Science and Technology, Beijing University of Chemical Technology, Beijing 100029, China;
2. State Key Laboratory of Bio-Based Fiber Manufacturing Technology, China Textile Academy, Beijing 100025, China;
3. Paris Curie Engineer School, Beijing University of Chemical Technology, Beijing 100029, China

Received:2024-01-10 Revised:2024-06-01 Accepted:2024-06-03 Online:2024-09-28 Published:2024-12-28
Contact: Peiyong Qin,E-mail:qinpeiyong@tsinghua.org.cn
Supported by:
This work was funded by National Natural Science Foundation of China (22278023), Beijing Municipal Science and Technology Planning Project (Z221100002722002), Beijing Natural Science Foundation (2222015) and the long-term from the Ministry of Finance and the Ministry of Education of China.

A covalently integrated ZIF-8/polyamide acid mixed matrix membrane with superior gas separation performance

Guozhen Li^1,2, Shiqi Ling^1,3, Yuhui Cui¹, Shilong Dong¹, Tianyin Liu², Ting Li², Siyu Pang¹, Peiyong Qin¹

1. National Energy Research and Development Center for Biorefinery, College of Life Science and Technology, Beijing University of Chemical Technology, Beijing 100029, China;
2. State Key Laboratory of Bio-Based Fiber Manufacturing Technology, China Textile Academy, Beijing 100025, China;
3. Paris Curie Engineer School, Beijing University of Chemical Technology, Beijing 100029, China

通讯作者: Peiyong Qin,E-mail:qinpeiyong@tsinghua.org.cn
基金资助:
This work was funded by National Natural Science Foundation of China (22278023), Beijing Municipal Science and Technology Planning Project (Z221100002722002), Beijing Natural Science Foundation (2222015) and the long-term from the Ministry of Finance and the Ministry of Education of China.

Abstract

Abstract: Zeolitic imidazolate framework-8 (ZIF-8) is a typical filler used to fabricate mixed matrix membranes (MMMs) on account of its attractive advantage of high selective permeability for gas separation. However, the performance is usually affected by filler aggregation due to strong interactions among fillers and weak interactions between the polymer and fillers, However, the performance is usually affected by filler aggregation due to strong interactions among fillers and weak interactions between the polymer and fillers, which will lead to a decrease of selectivity and the performance of gas separation will be strongly influenced. Herein, we modified ZIF-8 with 3-amino-1,2,4-triazole to obtain ZIF-8-NH₂, Kapton polyamide acid was selected as the polymer matrix. Results showed that the ZIF-8-NH₂/Kapton MMMs has a good compatibility interface between ZIF-8 and Kapton because of the covalent bridging, even the filler loading up to 45% (mass). The 45% (mass) of ZIF-8-NH₂/Kapton membrane showed 297 barrer (1 barrer = 10^-10 cm³·cm·cm^-2·s^-1·cmHg^-1, 1 cmHg = 1333.22 Pa, standard temperature and pressure) of the permeability of H₂ and 43.9 and 62.2 of selectivities for H₂/N₂ and for H₂/CH₄, respectively, which are beyond the upper limit of Robeson 2008.

Key words: Polyamide acid, ZIF-8, Mixed matrix membrane, Gas separation

摘要： Zeolitic imidazolate framework-8 (ZIF-8) is a typical filler used to fabricate mixed matrix membranes (MMMs) on account of its attractive advantage of high selective permeability for gas separation. However, the performance is usually affected by filler aggregation due to strong interactions among fillers and weak interactions between the polymer and fillers, However, the performance is usually affected by filler aggregation due to strong interactions among fillers and weak interactions between the polymer and fillers, which will lead to a decrease of selectivity and the performance of gas separation will be strongly influenced. Herein, we modified ZIF-8 with 3-amino-1,2,4-triazole to obtain ZIF-8-NH₂, Kapton polyamide acid was selected as the polymer matrix. Results showed that the ZIF-8-NH₂/Kapton MMMs has a good compatibility interface between ZIF-8 and Kapton because of the covalent bridging, even the filler loading up to 45% (mass). The 45% (mass) of ZIF-8-NH₂/Kapton membrane showed 297 barrer (1 barrer = 10^-10 cm³·cm·cm^-2·s^-1·cmHg^-1, 1 cmHg = 1333.22 Pa, standard temperature and pressure) of the permeability of H₂ and 43.9 and 62.2 of selectivities for H₂/N₂ and for H₂/CH₄, respectively, which are beyond the upper limit of Robeson 2008.

关键词: Polyamide acid, ZIF-8, Mixed matrix membrane, Gas separation

Guozhen Li, Shiqi Ling, Yuhui Cui, Shilong Dong, Tianyin Liu, Ting Li, Siyu Pang, Peiyong Qin. A covalently integrated ZIF-8/polyamide acid mixed matrix membrane with superior gas separation performance[J]. Chinese Journal of Chemical Engineering, 2024, 76(12): 30-41.

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A covalently integrated ZIF-8/polyamide acid mixed matrix membrane with superior gas separation performance

A covalently integrated ZIF-8/polyamide acid mixed matrix membrane with superior gas separation performance

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