An efficient bifunctional Ni-Nb2O5 nanocatalysts for the hydrodeoxygenation of anisole

doi:10.1016/j.cjche.2022.07.009

Chinese Journal of Chemical Engineering ›› 2022, Vol. 49 ›› Issue (9): 187-197.DOI: 10.1016/j.cjche.2022.07.009

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An efficient bifunctional Ni-Nb₂O₅ nanocatalysts for the hydrodeoxygenation of anisole

Juan Xu^1,2, Ping Zhu³, Islam H. El Azab⁴, Ben Bin Xu⁵, Zhanhu Guo⁶, Ashraf Y. Elnaggar⁴, Gaber A.M. Mersal⁷, Xiangyi Liu², Yunfei Zhi¹, Zhiping Lin⁸, Hassan Algadi⁹, Shaoyun Shan¹

1. Faculty of Chemical Engineering, Kunming University of Science and Technology, Kunming 650500, China;
2. College of Chemical Engineering, Southwest Forestry University, Kunming 650224, China;
3. Yunnan Province Special Equipment Safety Inspection and Research Institute, Kunming 650228, China;
4. Department of Food Science and Nutrition, College of Science, Taif University, Taif 21944, Saudi Arabia;
5. Department of Mechanical and Construction Engineering, Faculty of Engineering and Environment, Northumbria University, Newcastle upon Tyne NE1 8ST, UK;
6. Integrated Composites Lab (ICL), Department of Chemical & Biomolecular Engineering, University of Tennessee, Knoxville, TN 37996, USA;
7. Department of Chemistry, College of Science, Taif University, Taif 21944, Saudi Arabia;
8. Taizhou University, Taizhou 31800, China;
9. Department of Electrical Engineering, Faculty of Engineering, Najran University, Najran 11001, Saudi Arabia

Received:2022-03-05 Revised:2022-07-12 Online:2022-10-19
Contact: Zhanhu Guo,E-mail:nanomaterials2000@gmail.com;Shaoyun Shan,E-mail:shansy411@163.com
Supported by:
The authors acknowledge Major Science and Technology Project of Yunnan Province (202102AE090042), National Natural Science Foundation of China (21766016) and the Science and Technology Talent and Platform Program of Yunnan Provincial Science and Technology Department (202005AF150037). The authors acknowledge the financial support of Taif University Researchers Supporting Project (TURSP-2020/27), Taif University, Taif, Saudi Arabia.

An efficient bifunctional Ni-Nb₂O₅ nanocatalysts for the hydrodeoxygenation of anisole

Juan Xu^1,2, Ping Zhu³, Islam H. El Azab⁴, Ben Bin Xu⁵, Zhanhu Guo⁶, Ashraf Y. Elnaggar⁴, Gaber A.M. Mersal⁷, Xiangyi Liu², Yunfei Zhi¹, Zhiping Lin⁸, Hassan Algadi⁹, Shaoyun Shan¹

1. Faculty of Chemical Engineering, Kunming University of Science and Technology, Kunming 650500, China;
2. College of Chemical Engineering, Southwest Forestry University, Kunming 650224, China;
3. Yunnan Province Special Equipment Safety Inspection and Research Institute, Kunming 650228, China;
4. Department of Food Science and Nutrition, College of Science, Taif University, Taif 21944, Saudi Arabia;
5. Department of Mechanical and Construction Engineering, Faculty of Engineering and Environment, Northumbria University, Newcastle upon Tyne NE1 8ST, UK;
6. Integrated Composites Lab (ICL), Department of Chemical & Biomolecular Engineering, University of Tennessee, Knoxville, TN 37996, USA;
7. Department of Chemistry, College of Science, Taif University, Taif 21944, Saudi Arabia;
8. Taizhou University, Taizhou 31800, China;
9. Department of Electrical Engineering, Faculty of Engineering, Najran University, Najran 11001, Saudi Arabia

通讯作者: Zhanhu Guo,E-mail:nanomaterials2000@gmail.com;Shaoyun Shan,E-mail:shansy411@163.com
基金资助:
The authors acknowledge Major Science and Technology Project of Yunnan Province (202102AE090042), National Natural Science Foundation of China (21766016) and the Science and Technology Talent and Platform Program of Yunnan Provincial Science and Technology Department (202005AF150037). The authors acknowledge the financial support of Taif University Researchers Supporting Project (TURSP-2020/27), Taif University, Taif, Saudi Arabia.

Abstract

Abstract: The Ni-Nb₂O₅ nanocatalysts have been prepared by the sol–gel method, and the catalytic hydrodeoxygenation (HDO) performance of anisole as model compound is studied. The results show that Nb exists as amorphous Nb₂O₅ species, which can promote Ni dispersion. The addition of Nb₂O₅ increases the acidity of the catalyst. However, when the content of niobium is high, there is an inactive Nb-Ni-O mixed phase. The size and morphology of Ni grains in catalysts are different due to the difference of Nb/Ni molar ratio. The Ni_0.9Nb_0.1 sample has the largest surface area of 170.8 m²·g^-1 among the catalysts prepared in different Nb/Ni molar ratios, which is mainly composed of spherical nanoparticles and crack pores. The HDO of anisole follows the reaction route of the hydrogenation HYD route. The Ni_0.9Nb_0.1 catalyst displayed a higher HDO performance for anisole than Ni catalyst. The selectivity to cyclohexane over the Ni_0.9Nb_0.1 sample is about 10 times that of Ni catalyst at 220 ℃ and 3 MPa H₂. The selectivity of cyclohexane is increased with the increase of reaction temperature. The anisole is almost completely transformed into cyclohexane at 240 ℃, 3 MPa H₂ and 4 h.

Key words: Hydrodeoxygenation (HDO), Catalysts, Ni-Nb₂O₅, Sol–gel method, Anisole

摘要： The Ni-Nb₂O₅ nanocatalysts have been prepared by the sol–gel method, and the catalytic hydrodeoxygenation (HDO) performance of anisole as model compound is studied. The results show that Nb exists as amorphous Nb₂O₅ species, which can promote Ni dispersion. The addition of Nb₂O₅ increases the acidity of the catalyst. However, when the content of niobium is high, there is an inactive Nb-Ni-O mixed phase. The size and morphology of Ni grains in catalysts are different due to the difference of Nb/Ni molar ratio. The Ni_0.9Nb_0.1 sample has the largest surface area of 170.8 m²·g^-1 among the catalysts prepared in different Nb/Ni molar ratios, which is mainly composed of spherical nanoparticles and crack pores. The HDO of anisole follows the reaction route of the hydrogenation HYD route. The Ni_0.9Nb_0.1 catalyst displayed a higher HDO performance for anisole than Ni catalyst. The selectivity to cyclohexane over the Ni_0.9Nb_0.1 sample is about 10 times that of Ni catalyst at 220 ℃ and 3 MPa H₂. The selectivity of cyclohexane is increased with the increase of reaction temperature. The anisole is almost completely transformed into cyclohexane at 240 ℃, 3 MPa H₂ and 4 h.

关键词: Hydrodeoxygenation (HDO), Catalysts, Ni-Nb₂O₅, Sol–gel method, Anisole

Juan Xu, Ping Zhu, Islam H. El Azab, Ben Bin Xu, Zhanhu Guo, Ashraf Y. Elnaggar, Gaber A.M. Mersal, Xiangyi Liu, Yunfei Zhi, Zhiping Lin, Hassan Algadi, Shaoyun Shan. An efficient bifunctional Ni-Nb₂O₅ nanocatalysts for the hydrodeoxygenation of anisole[J]. Chinese Journal of Chemical Engineering, 2022, 49(9): 187-197.

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An efficient bifunctional Ni-Nb₂O₅ nanocatalysts for the hydrodeoxygenation of anisole

An efficient bifunctional Ni-Nb₂O₅ nanocatalysts for the hydrodeoxygenation of anisole

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