A two-stage blade-packing rotating packed bed for intensification of continuous distillation

doi:10.1016/j.cjche.2015.06.015

Chinese Journal of Chemical Engineering ›› 2016, Vol. 24 ›› Issue (1): 109-115.DOI: 10.1016/j.cjche.2015.06.015

• 第25届中国过程控制会议专栏 • 上一篇下一篇

A two-stage blade-packing rotating packed bed for intensification of continuous distillation

Yong Luo¹, Guangwen Chu¹, Le Sang¹, Haikui Zou¹, Yang Xiang¹, Jianfeng Chen^1,2

1 Research Center of the Ministry of Education for High Gravity Engineering and Technology, Beijing University of Chemical Technology, Beijing 100029, China;
2 State Key Laboratory of Organic-Inorganic Composites, Beijing University of Chemical Technology, Beijing 100029, China

收稿日期:2014-11-19 修回日期:2015-05-09 出版日期:2016-01-28 发布日期:2016-02-23
通讯作者: Guangwen Chu, Jianfeng Chen
基金资助:
Supported by the Fundamental Research Funds for the Central Universities (ZY1403), and the National Natural Science Foundation of China (No. 21406008 and No. U1462127).

A two-stage blade-packing rotating packed bed for intensification of continuous distillation

Yong Luo¹, Guangwen Chu¹, Le Sang¹, Haikui Zou¹, Yang Xiang¹, Jianfeng Chen^1,2

1 Research Center of the Ministry of Education for High Gravity Engineering and Technology, Beijing University of Chemical Technology, Beijing 100029, China;
2 State Key Laboratory of Organic-Inorganic Composites, Beijing University of Chemical Technology, Beijing 100029, China

Received:2014-11-19 Revised:2015-05-09 Online:2016-01-28 Published:2016-02-23
Contact: Guangwen Chu, Jianfeng Chen
Supported by:
Supported by the Fundamental Research Funds for the Central Universities (ZY1403), and the National Natural Science Foundation of China (No. 21406008 and No. U1462127).

摘要/Abstract

摘要： A two-stage blade-packing rotating packed bed (TSBP-RPB) was designed and developed for the intensification of continuous distillation. The mass transfer parameters of the TSBP-RPBwere investigated using a chemisorption system. Continuous distillation experiments were conducted in the TSBP-RPB by the methanol-water binary system. Experimental results showed that values of the effective interfacial area and liquid-side mass transfer coefficient of the TSBP-RPB were 93-337 m²·m^-3 and 0.05-0.19 cm·s^-1, respectively. The height of equivalent theoretical plate (HETP) of the TSBP-RPB ranged from 1.9 to 10 cm. Moreover, the TSBP-RPB is easy to be manufactured, which shows great potential for the application of continuous distillation.

关键词: Two-stage blade-packing rotating packed bed, Mass transfer, Distillation

Abstract: A two-stage blade-packing rotating packed bed (TSBP-RPB) was designed and developed for the intensification of continuous distillation. The mass transfer parameters of the TSBP-RPBwere investigated using a chemisorption system. Continuous distillation experiments were conducted in the TSBP-RPB by the methanol-water binary system. Experimental results showed that values of the effective interfacial area and liquid-side mass transfer coefficient of the TSBP-RPB were 93-337 m²·m^-3 and 0.05-0.19 cm·s^-1, respectively. The height of equivalent theoretical plate (HETP) of the TSBP-RPB ranged from 1.9 to 10 cm. Moreover, the TSBP-RPB is easy to be manufactured, which shows great potential for the application of continuous distillation.

Key words: Two-stage blade-packing rotating packed bed, Mass transfer, Distillation

Yong Luo, Guangwen Chu, Le Sang, Haikui Zou, Yang Xiang, Jianfeng Chen. A two-stage blade-packing rotating packed bed for intensification of continuous distillation[J]. Chinese Journal of Chemical Engineering, 2016, 24(1): 109-115.

参考文献

[1] A.I. Stankiewicz, J.A. Moulijn, Process intensification: Transforming chemical engineering, Chem. Eng. Prog. 11 (2000) 22-34.

[2] C. Ramshaw, R.H. Mallinson, Mass transfer apparatus and its use, European Patent, 0002568, 1979.

[3] D.P. Rao, A. Bhowal, P.S. Goswami, Process intensification in rotating packed beds (HIGEE): an appraisal, Ind. Eng. Chem. Res. 43 (2004) 1150-1162.

[4] W. Wang, H.K. Zou, G.W. Chu, Z. Weng, J.F. Chen, Bromination of butyl rubber in rotating packed bed reactor, Chem. Eng. J. 240 (2014) 503-508.

[5] H. Zhao, L. Shao, J.F. Chen, High-gravity process intensification technology and application, Chem. Eng. J. 156 (2010) 588-593.

[6] H. Llerena-Chavez, F. Larachi, Analysis of flow in rotating packed beds via CFD simulations—dry pressure drop and gas flow maldistribution, Chem. Eng. Sci. 64 (2009) 2113-2126.

[7] C. Ramshaw, R. H. Mallinson, Mass transfer process, US patent, 4283255, 1981.

[8] W.W. James, Centrifugal gas-liquid contact apparatus, US patent, 4382045, 1983.

[9] W.W. James, Centrifugal gas-liquid contact apparatus, US patent, 4382900, 1983.

[10] W.D. Sung, Y.S. Chen, Characteristics of a rotating packed bed equipped with blade packings and baffles, Sep. Purif. Technol. 93 (2012) 52-58.

[11] L.L. Zhang, J.X.Wang, Z.P. Liu, Y. Lu, G.W. Chu,W.C. Wang, J.F. Chen, Efficient capture of carbon dioxidewith novelmass-transfer intensification device using ionic liquids, AICHE J. 59 (2013) 6957-6964.

[12] K. Guo, Z.Z. Zhang, H.J. Luo, J.X. Dang, Z. Qian, An innovative approach of the effective mass transfer area in the rotating packed bed, Ind. Eng. Chem. Res. 53 (2014) 4052-4058.

[13] C. Ramshaw, HIGEE distillations—an example of process intensification, Chem. Eng. 389 (1983) 13-14.

[14] T. Kelleher, J.R. Fair, Distillation studies on a high-gravity gas-liquid contactor, Ind. Eng. Chem. Res. 35 (1996) 4646-4655.

[15] C.C. Lin, T.J. Ho, W.T. Liu, Distillation in a rotating packed bed, J. Chem. Eng. Jpn 35 (2002) 1298-1304.

[16] J.V.S. Nascimento, T.M.K. Ravagnani, J.A.F.R. Pereira, Experimental study of a rotating packed bed distillation column, Braz. J. Chem. Eng. 26 (2009) 219-226.

[17] A. Mondal, A. Pramanik, A. Bhowal, S. Datta, Distillation studies in rotating packed bed with split packing, Chem. Eng. Res. Des. 90 (2012) 453-457.

[18] H. Short, Newmass-transfer find is a matter of gravity, Chem. Eng. 90 (1983) 23-29.

[19] X.P. Li, Y.Z. Liu, Z.Q. Li, X. Wang, Continuous distillation experiment with rotating packed bed, Chin. J. Chem. Eng. 16 (2008) 656-662.

[20] G.Q. Wang, Z.C. Xu, Y.L. Yu, J.B. Ji, Performance of a rotating zigzag bed—A new HIGEE, Chem. Eng. Process. 47 (2008) 2131-2139.

[21] Y.M. Li, X.H. Li, Y.Wang, Y.Y. Chen, J.B. Ji, Y.L. Yu, Z.C. Xu, Distillation in a counterflow concentric-ring rotating bed, Ind. Eng. Chem. Res. 53 (2014) 4821-4837.

[22] Y. Luo, G.W. Chu, H.K. Zou, Y. Xiang, L. Shao, J.F. Chen, Characteristics of a two-stage counter-current rotating packed bed for continuous distillation, Chem. Eng. Process. 52 (2012) 55-62.

[23] G.W. Chu, X. Gao, Y. Luo, H.K. Zou, L. Shao, J.F. Chen, Distillation studies in a twostage counter-current rotating packed bed, Sep. Purif. Technol. 102 (2013) 62-66.

[24] J.R. Burns, C. Ramshaw, Process intensification: Visual study of liquid maldistribution in rotating packed beds, Chem. Eng. Sci. 51 (1996) 1347-1352.

[25] Y. Luo, G.W. Chu, H.K. Zou, F. Wang, Y. Xiang, L. Shao, J.F. Chen,Mass transfer studies in a rotating packed bed with novel rotors: Chemisorption of CO₂, Ind. Eng. Chem. Res. 51 (2012) 9164-9172.

[26] F. Guo, C. Zheng, K. Guo, Y.D. Feng, C.G. Nelson, Hydrodynamics andmass transfer in cross-flow rotating packed beds, Chem. Eng. Sci. 52 (1997) 3853-3859.

[27] K. Yang, G.W. Chu, H.K. Zou, B.C. Sun, L. Shao, J.F. Chen, Determination of the effective interfacial area in rotating packed bed, Chem. Eng. J. 168 (2011) 1377-1382.

[28] L.L. Zhang, J.X. Wang, Y. Xiang, X.F. Zeng, J.F. Chen, Absorption of carbon dioxide with ionic liquid in a rotating packed bed contactor: Mass transfer study, Ind. Eng. Chem. Res. 50 (2011) 6957-6964.

[29] Z.C. Xu, Y.L. Yu, J.B. Ji, Rotating zigzag high-gravity bed and its application in distillation, Petrochem. Technol. 34 (2005) 778-781 (in Chinese).

A two-stage blade-packing rotating packed bed for intensification of continuous distillation

A two-stage blade-packing rotating packed bed for intensification of continuous distillation

PDF (PC)

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价

[1]	Bo Yu, Guang Fu, Xinpei Li, Libo Zhang, Jing Li, Hongtao Qu, Dongbin Wang, Qingfeng Dong, Mengmeng Zhang. Arsenic removal from acidic industrial wastewater by ultrasonic activated phosphorus pentasulfide[J]. 中国化学工程学报, 2023, 60(8): 46-52.
[2]	Anjun Liu, Jie Chen, Meng Guo, Chengmin Chen, Meihong Yang, Chao Yang. The internal circulations on internal mass transfer rate of a single drop in nonlinear uniaxial extensional flow[J]. 中国化学工程学报, 2023, 59(7): 51-60.
[3]	Yingxi Gao, Jiayi Shi, Jie Wang, Fan Zhang, Shichao Tian, Zhiyong Zhou, Zhongqi Ren. Enrichment of nervonic acid in Acer truncatum Bunge oil by combination of two-stage molecular distillation, one-stage urea complexation and five-stage solvent crystallization[J]. 中国化学工程学报, 2023, 59(7): 61-71.
[4]	Kejin Huang, Shuaishuai Han, Lijing Zang, Haisheng Chen, Yihang Luo, Liang Zhang, Yang Yuan, Xing Qian, Shaofeng Wang. Configuring topologically optimum vapor recompressed dividing-wall distillation columns to maximize operating efficiency[J]. 中国化学工程学报, 2023, 57(5): 247-264.
[5]	Ming Chen, Huiyan Jiao, Jun Li, Zhibin Wang, Feng He, Yang Jin. Liquid–liquid two-phase flow in a wire-embedded concentric microchannel: Flow pattern and mass transfer performance[J]. 中国化学工程学报, 2023, 56(4): 281-289.
[6]	Wen Tian, Junyi Ji, Hongjiao Li, Changjun Liu, Lei Song, Kui Ma, Siyang Tang, Shan Zhong, Hairong Yue, Bin Liang. Measurements of the effective mass transfer areas for the gas–liquid rotating packed bed[J]. 中国化学工程学报, 2023, 55(3): 13-19.
[7]	Xinhao Li, Qing Ye, Jinlong Li, Lingqiang Yan, Xue Jian, Licheng Xie, Jianyu Zhang. Investigation of energy-efficient heat pump assisted heterogeneous azeotropic distillation for separating of acetonitrile/ethyl acetate/n-hexane mixture[J]. 中国化学工程学报, 2023, 55(3): 20-33.
[8]	Qi Han, Xin-Yuan Zhang, Hai-Bo Wu, Xian-Tai Zhou, Hong-Bing Ji. Different efficiency toward the biomimetic aerobic oxidation of benzyl alcohol in microchannel and bubble column reactors: Hydrodynamic characteristics and gas–liquid mass transfer[J]. 中国化学工程学报, 2023, 55(3): 84-92.
[9]	Qinyan Wang, Yang Jin, Jun Li, Yongbo Zhou, Ming Chen. Study on liquid–liquid two-phase mass transfer characteristics in the microchannel with deformed insert[J]. 中国化学工程学报, 2023, 54(2): 114-126.
[10]	Wei Qin, Lijing Zang, Kejin Huang, Haisheng Chen, Yang Yuan, Xing Qian, Liang Zhang, Shaofeng Wang. Reinforced temperature control of a reactive double dividing-wall distillation column[J]. 中国化学工程学报, 2023, 54(2): 288-295.
[11]	Qinggang Xu, Yasen Dai, Qing Zhao, Zhengrun Chen, Peizhe Cui, Zhaoyou Zhu, Yinglong Wang, Jun Gao, Yixin Ma. Economy, environmental assessment and energy conservation for separation of isopropanol/diisopropyl ether/water multi-azeotropes via extractive distillation coupled pervaporation process[J]. 中国化学工程学报, 2023, 54(2): 353-363.
[12]	Zhiwei Wang, Yu Zhang, Zhi Zhang, Daowei Zhou, Zhikai Cao, Yong Sha. Investigation on catalytic distillation for ethyl acetate production with different catalytic packing structures[J]. 中国化学工程学报, 2023, 53(1): 63-72.
[13]	Ting He, Songhong Yu, Jinhui He, Dejian Chen, Jie Li, Hongjun Hu, Xingrui Zhong, Yawei Wang, Zhaohui Wang, Zhaoliang Cui. Membranes for extracorporeal membrane oxygenator (ECMO): History, preparation, modification and mass transfer[J]. 中国化学工程学报, 2022, 49(9): 46-75.
[14]	Zhi-Guo Yuan, Yu-Xia Wang, You-Zhi Liu, Dan Wang, Wei-Zhou Jiao, Peng-Fei Liang. Research and development of advanced structured packing in a rotating packed bed[J]. 中国化学工程学报, 2022, 49(9): 178-186.
[15]	Xinqiang You, Kai Zhao, Ling Li, Ting Qiu. Ionic liquids as entrainer in extractive distillation for effectively separating 1-propanol–water azeotropic mixture[J]. 中国化学工程学报, 2022, 49(9): 224-233.