The Design and Control of Distillation Column with Side Reactors for Chlorobenzene Production*

Chinese Journal of Chemical Engineering ›› 2012, Vol. 20 ›› Issue (6): 1113-1120.

The Design and Control of Distillation Column with Side Reactors for Chlorobenzene Production^*

薄翠梅^1,2, 汤吉海², 柏杨进¹, 乔旭², 丁良辉², 张湜¹

1. College of Automation and Electrical Engineering, Nanjing University of Technology, Nanjing 210009, China;
2. State Key Laboratory of Materials-oriented Chemical Engineering, Nanjing University of Technology, Nanjing 210009, China

收稿日期:2012-05-28 修回日期:2012-07-20 出版日期:2012-12-28 发布日期:2012-12-28
通讯作者: BO Cuimei,E-mail:qct@njut.edu.cn;lj_bcm@163.com
基金资助:
Supported by the National Natural Science Foundation of China (61203020;21276126);the Natural Science Foundation of Jiangsu Province (BK2011795);Jiangsu Province Higher Education Natural Science Foundation (09KJA530004);China Postdoctoral Science Foundation (20100471325)

The Design and Control of Distillation Column with Side Reactors for Chlorobenzene Production^*

BO Cuimei^1,2, TANG Jihai², BAI Yangjin¹, QIAO Xu², DING Lianghui², ZHANG Shi¹

1. College of Automation and Electrical Engineering, Nanjing University of Technology, Nanjing 210009, China;
2. State Key Laboratory of Materials-oriented Chemical Engineering, Nanjing University of Technology, Nanjing 210009, China

Received:2012-05-28 Revised:2012-07-20 Online:2012-12-28 Published:2012-12-28
Supported by:
Supported by the National Natural Science Foundation of China (61203020;21276126);the Natural Science Foundation of Jiangsu Province (BK2011795);Jiangsu Province Higher Education Natural Science Foundation (09KJA530004);China Postdoctoral Science Foundation (20100471325)

摘要/Abstract

摘要： The distillation column with side reactors (SRC) can overcome the temperature/pressure mismatch in the traditional reactive distillation,the column operates at temperature/pressure favorable for vapor-liquid separation,while the reactors operate at temperatures/pressures favorable for reaction kinetics.According to the smooth operation and automatic control problem of the distillation column with side reactors (SRC),the design,simulation calculation and dynamic control of the SCR process for chlorobenzene production are discussed in the paper.Firstly,the mechanism models,the integrated structure optimal design and process simulation systems are established,respectively.And then multivariable control schemes are designed,the controllability of SRC process based on the optimal steady-state integrated structure is explored.The dynamic response performances of closed-loop system against several disturbances are discussed to verify the effectiveness of control schemes for the SRC process.The simulating results show that the control structure using conventional control strategies can effectively overcome feeding disturbances in a specific range.

关键词: distillation column with side reactors (SRC), mechanism models, multivariable control schemes, simulation system, chlorobenzene production

Abstract: The distillation column with side reactors (SRC) can overcome the temperature/pressure mismatch in the traditional reactive distillation,the column operates at temperature/pressure favorable for vapor-liquid separation,while the reactors operate at temperatures/pressures favorable for reaction kinetics.According to the smooth operation and automatic control problem of the distillation column with side reactors (SRC),the design,simulation calculation and dynamic control of the SCR process for chlorobenzene production are discussed in the paper.Firstly,the mechanism models,the integrated structure optimal design and process simulation systems are established,respectively.And then multivariable control schemes are designed,the controllability of SRC process based on the optimal steady-state integrated structure is explored.The dynamic response performances of closed-loop system against several disturbances are discussed to verify the effectiveness of control schemes for the SRC process.The simulating results show that the control structure using conventional control strategies can effectively overcome feeding disturbances in a specific range.

Key words: distillation column with side reactors (SRC), mechanism models, multivariable control schemes, simulation system, chlorobenzene production

薄翠梅, 汤吉海, 柏杨进, 乔旭, 丁良辉, 张湜. The Design and Control of Distillation Column with Side Reactors for Chlorobenzene Production^*[J]. Chinese Journal of Chemical Engineering, 2012, 20(6): 1113-1120.

BO Cuimei, TANG Jihai, BAI Yangjin, QIAO Xu, DING Lianghui, ZHANG Shi. The Design and Control of Distillation Column with Side Reactors for Chlorobenzene Production^*[J]. Chin.J.Chem.Eng., 2012, 20(6): 1113-1120.

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[1]	Cuimei Bo, Jun Li, Lei Yang, Hui Yi, Jihai Tang, Xu Qiao. MPC of distillation column with side reactors for methyl acetate[J]. Chinese Journal of Chemical Engineering, 2017, 25(12): 1798-1804.
[2]	罗春鹏, 荣冈. A Strategy for the Integration of Production Planning and Scheduling in Refineries under Uncertainty[J]. , 2009, 17(1): 113-127.

The Design and Control of Distillation Column with Side Reactors for Chlorobenzene Production^*

The Design and Control of Distillation Column with Side Reactors for Chlorobenzene Production^*

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