In-depth investigation on the factors affecting the performance of high oil-absorption resin by response surface method

doi:10.1016/j.cjche.2020.07.032

Chinese Journal of Chemical Engineering ›› 2021, Vol. 33 ›› Issue (5): 286-296.DOI: 10.1016/j.cjche.2020.07.032

In-depth investigation on the factors affecting the performance of high oil-absorption resin by response surface method

Lei Ma¹, Hongxia Lv¹, Haonan Yu¹, Lingtong Kong¹, Rongyue Zhang¹, Xiaoyan Guo¹, Haibo Jin¹, Guangxiang He¹, Xiaoyan Liu²

1 Beijing Key Laboratory of Fuels Cleaning and Advanced Catalytic Emission Reduction Technology, College of Chemical Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617,;
China;
2 Water Resource Office of Jining City, Shandong Province, Jining 272019, China

Received:2020-03-20 Revised:2020-07-09 Online:2021-08-19 Published:2021-05-28
Contact: Haibo Jin, Guangxiang He
Supported by:
This work was funded by Project of Construction of Innovative Teams and Teacher Career Development for Universities and Colleges under Beijing Municipality (IDHT20180508), Scientific Research Common Program of Beijing Municipal Commission of Education (KM202010017006), the Talents Project of Beijing Organization Department (2018000020124G091), the Strategic Priority Research Program of the Chinese Academy of Sciences (XDA21021101) and the National Key Research and Development Program of China (2019YFA0705803).

In-depth investigation on the factors affecting the performance of high oil-absorption resin by response surface method

Lei Ma¹, Hongxia Lv¹, Haonan Yu¹, Lingtong Kong¹, Rongyue Zhang¹, Xiaoyan Guo¹, Haibo Jin¹, Guangxiang He¹, Xiaoyan Liu²

1 Beijing Key Laboratory of Fuels Cleaning and Advanced Catalytic Emission Reduction Technology, College of Chemical Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617,;
China;
2 Water Resource Office of Jining City, Shandong Province, Jining 272019, China

通讯作者: Haibo Jin, Guangxiang He
基金资助:
This work was funded by Project of Construction of Innovative Teams and Teacher Career Development for Universities and Colleges under Beijing Municipality (IDHT20180508), Scientific Research Common Program of Beijing Municipal Commission of Education (KM202010017006), the Talents Project of Beijing Organization Department (2018000020124G091), the Strategic Priority Research Program of the Chinese Academy of Sciences (XDA21021101) and the National Key Research and Development Program of China (2019YFA0705803).

Abstract

Abstract: A series of high oil-absorption resins with low cross-linking degree were synthesized by suspension polymerization using stearyl methacrylate (SMA), 2-Ethylhexyl methacrylate (EHMA), and styrene (St) as monomers. Response surface methodology (RSM) with central composite design (CCD) was also applied to determine the optimal parameters that are mainly known to affect their synthesis. Thus, the effects of the monomer mass ratio (EHMA:SMA), the rigid monomer (St) dosage, the porous agent (acetone) dosage, and their pairwise interaction on the resin's oil-absorption capacity were analyzed, highlighting PSES-R2 as the resin with the optimum performance. The pure oil-absorption rates of PSES-R₂ for gasoline, diesel, and kerosene were 11.19 g·g^-1, 16.25 g·g^-1, and 14.84 g·g^-1, respectively, while the oil removal rates from oily wastewater were 98.82%, 65.11%, and 99.63%, respectively.

Key words: Oil-absorption resin, Response surface method, Oil removal rate, Waste water, Absorption, Polymerization

摘要： A series of high oil-absorption resins with low cross-linking degree were synthesized by suspension polymerization using stearyl methacrylate (SMA), 2-Ethylhexyl methacrylate (EHMA), and styrene (St) as monomers. Response surface methodology (RSM) with central composite design (CCD) was also applied to determine the optimal parameters that are mainly known to affect their synthesis. Thus, the effects of the monomer mass ratio (EHMA:SMA), the rigid monomer (St) dosage, the porous agent (acetone) dosage, and their pairwise interaction on the resin's oil-absorption capacity were analyzed, highlighting PSES-R2 as the resin with the optimum performance. The pure oil-absorption rates of PSES-R₂ for gasoline, diesel, and kerosene were 11.19 g·g^-1, 16.25 g·g^-1, and 14.84 g·g^-1, respectively, while the oil removal rates from oily wastewater were 98.82%, 65.11%, and 99.63%, respectively.

关键词: Oil-absorption resin, Response surface method, Oil removal rate, Waste water, Absorption, Polymerization

Lei Ma, Hongxia Lv, Haonan Yu, Lingtong Kong, Rongyue Zhang, Xiaoyan Guo, Haibo Jin, Guangxiang He, Xiaoyan Liu. In-depth investigation on the factors affecting the performance of high oil-absorption resin by response surface method[J]. Chinese Journal of Chemical Engineering, 2021, 33(5): 286-296.

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In-depth investigation on the factors affecting the performance of high oil-absorption resin by response surface method

In-depth investigation on the factors affecting the performance of high oil-absorption resin by response surface method

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