A simple plasma reduction for synthesis of Au and Pd nanoparticles at room temperature

doi:10.1016/j.cjche.2014.09.055

Chinese Journal of Chemical Engineering ›› 2015, Vol. 23 ›› Issue (6): 1060-1063.DOI: 10.1016/j.cjche.2014.09.055

• 研究简报 • 上一篇

A simple plasma reduction for synthesis of Au and Pd nanoparticles at room temperature

Zhao Wang, Yu Zhu

State Key Laboratory of Chemical Engineering, School of Chemical Engineering, Tianjin University, Tianjin 300072, China

收稿日期:2014-05-05 修回日期:2014-09-04 出版日期:2015-06-28 发布日期:2015-07-09
通讯作者: Zhao Wang
基金资助:
Supported by the National Natural Science Foundation of China (21206109) and the Tianjin Municipal Natural Science Foundation (12JCQNJC04500).

A simple plasma reduction for synthesis of Au and Pd nanoparticles at room temperature

Zhao Wang, Yu Zhu

State Key Laboratory of Chemical Engineering, School of Chemical Engineering, Tianjin University, Tianjin 300072, China

Received:2014-05-05 Revised:2014-09-04 Online:2015-06-28 Published:2015-07-09
Contact: Zhao Wang
Supported by:
Supported by the National Natural Science Foundation of China (21206109) and the Tianjin Municipal Natural Science Foundation (12JCQNJC04500).

摘要/Abstract

摘要： A simple and fast plasma reduction method is developed for synthesis of Au and Pd metal nanoparticles. The scanning electron microscopy (SEM) analysis indicates a formation of aggregates of Au and Pd nanoparticles with branched structure. The transmission electron microscopy (TEM) image shows that the inclusive nanoparticles are all about 5 nm in size. Compared to conventional hydrogen reduction method, plasmamethod inhibits the agglomeration of metal particles. The room temperature operation is very helpful to limit the nanoparticle size. Most interestingly, plasma reduction produces more flattened metal particles. This plasma reduction does not require the use of any hazardous reducing chemicals, showing the great potential for the fabrication of noble metal nanoparticles.

关键词: Glow discharge plasma, Nanoparticles, Gold, Palladium, Reduction, Preparation

Abstract: A simple and fast plasma reduction method is developed for synthesis of Au and Pd metal nanoparticles. The scanning electron microscopy (SEM) analysis indicates a formation of aggregates of Au and Pd nanoparticles with branched structure. The transmission electron microscopy (TEM) image shows that the inclusive nanoparticles are all about 5 nm in size. Compared to conventional hydrogen reduction method, plasmamethod inhibits the agglomeration of metal particles. The room temperature operation is very helpful to limit the nanoparticle size. Most interestingly, plasma reduction produces more flattened metal particles. This plasma reduction does not require the use of any hazardous reducing chemicals, showing the great potential for the fabrication of noble metal nanoparticles.

Key words: Glow discharge plasma, Nanoparticles, Gold, Palladium, Reduction, Preparation

Zhao Wang, Yu Zhu. A simple plasma reduction for synthesis of Au and Pd nanoparticles at room temperature[J]. Chinese Journal of Chemical Engineering, 2015, 23(6): 1060-1063.

Zhao Wang, Yu Zhu. A simple plasma reduction for synthesis of Au and Pd nanoparticles at room temperature[J]. Chin.J.Chem.Eng., 2015, 23(6): 1060-1063.

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A simple plasma reduction for synthesis of Au and Pd nanoparticles at room temperature

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