Experimental measurement and thermodynamic modeling of binary and ternary solid-liquid phase equilibrium for the systems formed by L-arabinose, D-xylose and water

doi:10.1016/j.cjche.2017.02.005

›› 2017, Vol. 25 ›› Issue (10): 1467-1472.DOI: 10.1016/j.cjche.2017.02.005

• Chemical Engineering Thermodynamics • 上一篇下一篇

Experimental measurement and thermodynamic modeling of binary and ternary solid-liquid phase equilibrium for the systems formed by L-arabinose, D-xylose and water

Lei Guo, Lianying Wu, Weitao Zhang, Chen Liang, Yangdong Hu

College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao 266100, China

收稿日期:2016-09-27 修回日期:2017-02-13 出版日期:2017-10-28 发布日期:2017-11-15
通讯作者: Yangdong Hu,E-mail address:ydhuhd@ouc.edu.cn
基金资助:
Supported by the National Natural Science Foundation of China (21376231).

Experimental measurement and thermodynamic modeling of binary and ternary solid-liquid phase equilibrium for the systems formed by L-arabinose, D-xylose and water

Lei Guo, Lianying Wu, Weitao Zhang, Chen Liang, Yangdong Hu

College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao 266100, China

Received:2016-09-27 Revised:2017-02-13 Online:2017-10-28 Published:2017-11-15
Supported by:
Supported by the National Natural Science Foundation of China (21376231).

摘要/Abstract

摘要： Solid-liquid phase equilibrium data for binary (L-arabinose-water) and (D-xylose-water) systems at temperatures from (269.85-298.05) K and ternary (L-arabinose-D-xylose-water) system at temperatures of 273.85 K, 278.85 K and 284.45 K were measured at atmospheric pressure. The ternary phase diagrams of the systems were constructed on the base of the measured solubility. Two pure solid phases were formed at given temperatures, including pure L-arabinose and pure D-xylose, which were confirmed and determined by the method of Schreinemakers' wet residue. At the same temperature, the crystallization region of L-arabinose was larger than D-xylose's. The acquired solubility data were then correlated using the NRTL model, Wilson model and Xu model. The calculated solubility with the three models agreed well with the experimental values.

关键词: D-Xylose, L-Arabinose, Solid-liquid equilibrium, Solubility, Thermodynamics, Model

Abstract: Solid-liquid phase equilibrium data for binary (L-arabinose-water) and (D-xylose-water) systems at temperatures from (269.85-298.05) K and ternary (L-arabinose-D-xylose-water) system at temperatures of 273.85 K, 278.85 K and 284.45 K were measured at atmospheric pressure. The ternary phase diagrams of the systems were constructed on the base of the measured solubility. Two pure solid phases were formed at given temperatures, including pure L-arabinose and pure D-xylose, which were confirmed and determined by the method of Schreinemakers' wet residue. At the same temperature, the crystallization region of L-arabinose was larger than D-xylose's. The acquired solubility data were then correlated using the NRTL model, Wilson model and Xu model. The calculated solubility with the three models agreed well with the experimental values.

Key words: D-Xylose, L-Arabinose, Solid-liquid equilibrium, Solubility, Thermodynamics, Model

Lei Guo, Lianying Wu, Weitao Zhang, Chen Liang, Yangdong Hu. Experimental measurement and thermodynamic modeling of binary and ternary solid-liquid phase equilibrium for the systems formed by L-arabinose, D-xylose and water[J]. , 2017, 25(10): 1467-1472.

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Experimental measurement and thermodynamic modeling of binary and ternary solid-liquid phase equilibrium for the systems formed by L-arabinose, D-xylose and water

Experimental measurement and thermodynamic modeling of binary and ternary solid-liquid phase equilibrium for the systems formed by L-arabinose, D-xylose and water

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