Highly dispersible cerium-oxide modified Ni/SBA-15 for steam reforming of bio-mass based JP10

doi:10.1016/j.cjche.2022.01.016

中国化学工程学报 ›› 2022, Vol. 43 ›› Issue (3): 255-265.DOI: 10.1016/j.cjche.2022.01.016

Highly dispersible cerium-oxide modified Ni/SBA-15 for steam reforming of bio-mass based JP10

Haocui Zhang¹, Zhourong Xiao¹, Mei Yang², Jijun Zou¹, Guozhu Liu¹, Xiangwen Zhang¹

1. Key Laboratory for Green Chemical Technology of Ministry of Education, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China;
2. Microchemical Engineering and Technology Group, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China

收稿日期:2021-08-30 修回日期:2021-12-14 出版日期:2022-03-28 发布日期:2022-04-28
通讯作者: Guozhu Liu,E-mail:gLiu@tju.edu.cn;Xiangwen Zhang,E-mail:zhangxiangwen@tju.edu.cn
基金资助:
The authors sincerely acknowledge financial support of the National Natural Science Foundation of China (21522605) and Tianjin Natural Science Foundation (Distinguish Young Scientist Program, Grant No. 18JCJQJC46800).

Highly dispersible cerium-oxide modified Ni/SBA-15 for steam reforming of bio-mass based JP10

Haocui Zhang¹, Zhourong Xiao¹, Mei Yang², Jijun Zou¹, Guozhu Liu¹, Xiangwen Zhang¹

1. Key Laboratory for Green Chemical Technology of Ministry of Education, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China;
2. Microchemical Engineering and Technology Group, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China

Received:2021-08-30 Revised:2021-12-14 Online:2022-03-28 Published:2022-04-28
Contact: Guozhu Liu,E-mail:gLiu@tju.edu.cn;Xiangwen Zhang,E-mail:zhangxiangwen@tju.edu.cn
Supported by:
The authors sincerely acknowledge financial support of the National Natural Science Foundation of China (21522605) and Tianjin Natural Science Foundation (Distinguish Young Scientist Program, Grant No. 18JCJQJC46800).

摘要/Abstract

摘要： Ni/SBA-15 modified by highly dispersed cerium-oxide was prepared with the aid of sucrose for steam reforming of JP10 (C₁₀H₁₆). Their characterization showed that addition of appropriate amount ceria led to the formation of highly dispersed CeO₂ and Ni, and the CeO₂ covered smaller nickel particles like strawberry seeds to form much more interface between them. Their catalytic activity exhibited higher stability over time on stream of 6.5 h with conversion higher than 95% and higher carbon resistance (mass loss less than 4.5% by TG), which may derive from good properties below: (1) much more interface enhanced cooperation effect and increased turnover frequency at the interface; (2) the stronger interaction between Ni and ceria to suppress sintering by formation of Ni-O-Ce solid solution; (3) the large amount of oxygen vacancies from the formation of Ni-O-Ce solid solution and highly dispersed CeO₂ to facilitate the water–gas–shift reaction and carbon removal.

关键词: JP-10, Steam reforming, Ceria, Nickel, Ni-CeO₂ cooperation

Abstract: Ni/SBA-15 modified by highly dispersed cerium-oxide was prepared with the aid of sucrose for steam reforming of JP10 (C₁₀H₁₆). Their characterization showed that addition of appropriate amount ceria led to the formation of highly dispersed CeO₂ and Ni, and the CeO₂ covered smaller nickel particles like strawberry seeds to form much more interface between them. Their catalytic activity exhibited higher stability over time on stream of 6.5 h with conversion higher than 95% and higher carbon resistance (mass loss less than 4.5% by TG), which may derive from good properties below: (1) much more interface enhanced cooperation effect and increased turnover frequency at the interface; (2) the stronger interaction between Ni and ceria to suppress sintering by formation of Ni-O-Ce solid solution; (3) the large amount of oxygen vacancies from the formation of Ni-O-Ce solid solution and highly dispersed CeO₂ to facilitate the water–gas–shift reaction and carbon removal.

Key words: JP-10, Steam reforming, Ceria, Nickel, Ni-CeO₂ cooperation

Haocui Zhang, Zhourong Xiao, Mei Yang, Jijun Zou, Guozhu Liu, Xiangwen Zhang. Highly dispersible cerium-oxide modified Ni/SBA-15 for steam reforming of bio-mass based JP10[J]. 中国化学工程学报, 2022, 43(3): 255-265.

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Highly dispersible cerium-oxide modified Ni/SBA-15 for steam reforming of bio-mass based JP10

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