Measurement and Correlation of Solubilities of C.I.Disperse Red 73, C. I. Disperse Blue 183 and Their Mixture in Supercritical Carbon Dioxide

›› 2010, Vol. 18 ›› Issue (4): 648-653.

Measurement and Correlation of Solubilities of C.I.Disperse Red 73, C. I. Disperse Blue 183 and Their Mixture in Supercritical Carbon Dioxide

郑金花¹, 徐明仙², 鲁雪燕¹, 林春绵¹

1. College of Biological and Environmental Engineering, Zhejiang University of Technology, Hangzhou 310014, China;
2. Department of Chemical Engineering, Hangzhou Vocational Technical College, Hangzhou 310018, China

收稿日期:2009-12-08 修回日期:2010-03-30 出版日期:2010-08-28 发布日期:2010-08-28
通讯作者: LIN Chunmian, E-mail:lcm@zjut.edu.cn
基金资助:
Supported by the Natural Science Foundation of Zhejiang Province(M203035)

Measurement and Correlation of Solubilities of C.I.Disperse Red 73, C. I. Disperse Blue 183 and Their Mixture in Supercritical Carbon Dioxide

ZHENG Jinhua¹, XU Mingxian², LU Xueyan1¹, LIN Chunmian¹

1. College of Biological and Environmental Engineering, Zhejiang University of Technology, Hangzhou 310014, China;
2. Department of Chemical Engineering, Hangzhou Vocational Technical College, Hangzhou 310018, China

Received:2009-12-08 Revised:2010-03-30 Online:2010-08-28 Published:2010-08-28

摘要/Abstract

摘要： The solubility of disperse dyes and their mixture in supercritical carbon dioxide is an important property in study and development of supercritical fluid dyeing technology.In this study,solubilities of C. I. Disperse Red 73,C.I.Disperse Blue 183 and their mixture in supercritical CO₂ are measured at temperatures from 343.2 to 383.2 K and pressures from 12 to 28 MPa with a static recirculation method.Under the experimental conditions for the binary(C. I.Disperse Red 73+CO₂ or C. I. Disperse Blue 183+CO₂) and ternary (C. I. Disperse Red 73+C. I. Disperse Blue 183+CO₂) systems,the solubilities increase with pressure.The solubility of C. I.Disperse Blue 183 decreases with the increase of temperature when the pressure is lower than 16 MPa,and the trend is opposite when the pressure is higher than 16 MPa.However,there is no crossover pressure for C.I.Disperse Red 73.The solubilities are also affected by molecular polarity of dyes.The co-solvent effect exhibited in the dissolving process of mixed dyes promotes their dissolution in supercritical CO₂ .The experimental data of solubilities of C. I.Disperse Red 73,C. I.Disperse Blue 183,and their mixture are correlated with the Chrastil model and Mendez-Santiago/Teja model. The former is more accurate.

关键词: supercritical CO₂ , solubility, Disperse Red 73, Disperse Blue 183

Abstract: The solubility of disperse dyes and their mixture in supercritical carbon dioxide is an important property in study and development of supercritical fluid dyeing technology.In this study,solubilities of C. I. Disperse Red 73,C.I.Disperse Blue 183 and their mixture in supercritical CO₂ are measured at temperatures from 343.2 to 383.2 K and pressures from 12 to 28 MPa with a static recirculation method.Under the experimental conditions for the binary(C. I.Disperse Red 73+CO₂ or C. I. Disperse Blue 183+CO₂) and ternary (C. I. Disperse Red 73+C. I. Disperse Blue 183+CO₂) systems,the solubilities increase with pressure.The solubility of C. I.Disperse Blue 183 decreases with the increase of temperature when the pressure is lower than 16 MPa,and the trend is opposite when the pressure is higher than 16 MPa.However,there is no crossover pressure for C.I.Disperse Red 73.The solubilities are also affected by molecular polarity of dyes.The co-solvent effect exhibited in the dissolving process of mixed dyes promotes their dissolution in supercritical CO₂ .The experimental data of solubilities of C. I.Disperse Red 73,C. I.Disperse Blue 183,and their mixture are correlated with the Chrastil model and Mendez-Santiago/Teja model. The former is more accurate.

Key words: supercritical CO₂ , solubility, Disperse Red 73, Disperse Blue 183

郑金花, 徐明仙, 鲁雪燕, 林春绵. Measurement and Correlation of Solubilities of C.I.Disperse Red 73, C. I. Disperse Blue 183 and Their Mixture in Supercritical Carbon Dioxide[J]. , 2010, 18(4): 648-653.

ZHENG Jinhua, XU Mingxian, LU Xueyan1, LIN Chunmian. Measurement and Correlation of Solubilities of C.I.Disperse Red 73, C. I. Disperse Blue 183 and Their Mixture in Supercritical Carbon Dioxide[J]. , 2010, 18(4): 648-653.

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Measurement and Correlation of Solubilities of C.I.Disperse Red 73, C. I. Disperse Blue 183 and Their Mixture in Supercritical Carbon Dioxide

Measurement and Correlation of Solubilities of C.I.Disperse Red 73, C. I. Disperse Blue 183 and Their Mixture in Supercritical Carbon Dioxide

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