Improved SSZ-13 thin membranes fabricated by seeded-gel approach for efficient CO2 capture

doi:10.1016/j.cjche.2022.07.012

中国化学工程学报 ›› 2023, Vol. 56 ›› Issue (4): 273-280.DOI: 10.1016/j.cjche.2022.07.012

• Full Length Article • 上一篇下一篇

Improved SSZ-13 thin membranes fabricated by seeded-gel approach for efficient CO₂ capture

Xingzhong Li, Kunlin Yu, Zibo He, Bo Liu, Rongfei Zhou, Weihong Xing

State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, Nanjing Tech University, Nanjing 210009, China

收稿日期:2022-04-10 修回日期:2022-07-12 出版日期:2023-04-28 发布日期:2023-06-13
通讯作者: Bo Liu,E-mail:liu@njtech.edu.cn;Rongfei Zhou,E-mail:rf-zhou@njtech.edu.cn
基金资助:
Financial supports from the National Natural Science Foundation of China (21921006, 21938007 and 21576131) and the open project of the State Key Laboratory of Materials-Oriented Chemical Engineering of China (KL21-04) are gratefully acknowledged.

Improved SSZ-13 thin membranes fabricated by seeded-gel approach for efficient CO₂ capture

Xingzhong Li, Kunlin Yu, Zibo He, Bo Liu, Rongfei Zhou, Weihong Xing

State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, Nanjing Tech University, Nanjing 210009, China

Received:2022-04-10 Revised:2022-07-12 Online:2023-04-28 Published:2023-06-13
Contact: Bo Liu,E-mail:liu@njtech.edu.cn;Rongfei Zhou,E-mail:rf-zhou@njtech.edu.cn
Supported by:
Financial supports from the National Natural Science Foundation of China (21921006, 21938007 and 21576131) and the open project of the State Key Laboratory of Materials-Oriented Chemical Engineering of China (KL21-04) are gratefully acknowledged.

摘要/Abstract

摘要： High-quality standard oil synthetic zeolite-13 (SSZ-13) membranes with thickness only ~ 1.0 μm were prepared on tubular supports by the new seeded-gel approach. Seeded-gel approach is simpler than the normal secondary-growth one since adding seeds in the gel is simpler than seeding on the support surface. The synthesis time was greatly reduced from 3.0 to 1.0 d after synthesis modification of gel aging and seed sizes. Low temperature ozone calcination was used for the removal of the organic structural directing agent. The best SSZ-13 membrane displayed CO₂ permeances of 1.3×10^–6 and 1.5×10^–6 mol·m^-2·s^-1·Pa^-1 and CO₂/CH₄ and CO₂/N₂ selectivities of 125 and 27 for equimolar CO₂/CH₄ and CO₂/N₂ mixtures at 0.2 MPa pressure drop and 298 K, respectively. Separation performance of the membrane in the two binary mixtures is higher than that of most zeolite membranes. Three SSZ-13 membranes were reproducibly prepared on tubular supports by seeded-gel approach and the standard deviation ratios of CO₂ permeance and CO₂/CH₄ selectivity are 12.5% and 7%, respectively. It suggests that this new synthesis approach is creditable. The effects of temperature and pressure on separation performance of the thin SSZ-13 membranes were studied in the two binary mixtures. The tubular SSZ-13 membranes displayed great potentials for CO₂ capture from natural gas, biogas and flue gas.

关键词: Zeolite CHA, Zeolite membranes, SSZ-13, Gas separation, CO₂ capture, Seeded-gel approach

Abstract: High-quality standard oil synthetic zeolite-13 (SSZ-13) membranes with thickness only ~ 1.0 μm were prepared on tubular supports by the new seeded-gel approach. Seeded-gel approach is simpler than the normal secondary-growth one since adding seeds in the gel is simpler than seeding on the support surface. The synthesis time was greatly reduced from 3.0 to 1.0 d after synthesis modification of gel aging and seed sizes. Low temperature ozone calcination was used for the removal of the organic structural directing agent. The best SSZ-13 membrane displayed CO₂ permeances of 1.3×10^–6 and 1.5×10^–6 mol·m^-2·s^-1·Pa^-1 and CO₂/CH₄ and CO₂/N₂ selectivities of 125 and 27 for equimolar CO₂/CH₄ and CO₂/N₂ mixtures at 0.2 MPa pressure drop and 298 K, respectively. Separation performance of the membrane in the two binary mixtures is higher than that of most zeolite membranes. Three SSZ-13 membranes were reproducibly prepared on tubular supports by seeded-gel approach and the standard deviation ratios of CO₂ permeance and CO₂/CH₄ selectivity are 12.5% and 7%, respectively. It suggests that this new synthesis approach is creditable. The effects of temperature and pressure on separation performance of the thin SSZ-13 membranes were studied in the two binary mixtures. The tubular SSZ-13 membranes displayed great potentials for CO₂ capture from natural gas, biogas and flue gas.

Key words: Zeolite CHA, Zeolite membranes, SSZ-13, Gas separation, CO₂ capture, Seeded-gel approach

Xingzhong Li, Kunlin Yu, Zibo He, Bo Liu, Rongfei Zhou, Weihong Xing. Improved SSZ-13 thin membranes fabricated by seeded-gel approach for efficient CO₂ capture[J]. 中国化学工程学报, 2023, 56(4): 273-280.

Xingzhong Li, Kunlin Yu, Zibo He, Bo Liu, Rongfei Zhou, Weihong Xing. Improved SSZ-13 thin membranes fabricated by seeded-gel approach for efficient CO₂ capture[J]. Chinese Journal of Chemical Engineering, 2023, 56(4): 273-280.

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Improved SSZ-13 thin membranes fabricated by seeded-gel approach for efficient CO₂ capture

Improved SSZ-13 thin membranes fabricated by seeded-gel approach for efficient CO₂ capture

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